Synthetic Route of 253-52-1, The reaction rate of a catalyzed reaction is faster than the reaction rate of the uncatalyzed reaction at the same temperature.253-52-1, Name is Phthalazine, molecular formula is C8H6N2. In a Article£¬once mentioned of 253-52-1
Self-assembly of ID- And 3D-networks through non-coordination intermodular forces: Synthesis and crystal structures of copper(I) complexes based on pyridazine-type ligands
Reaction of [Cu2(H3CCN)2(mu-pydz) 3][PF6]2 (1) with an excess of pyridazine or phthalazine yielded the novel dinuclear complexes [Cu2(mu-pydz) 3(pydz)2][PF6]2 (2) and [Cu 2(mupydz)(mu-phtz)2(phtz)2][PF 6]2 (5), respectively. Depolymerisation of the coordination polymer ?1{[Cu(mu-pydz) 2][PF6]} (3) in dichloromethane by addition of an excess of benzo[c]cinnoline afforded the dinuclear copper(I) salt [Cu 2(mu-pydz)2(pydz)2(benzo[c]cinnoline) 2][PF6]2 (4). Furthermore, a new route for the preparation of bis(benzonitrile)tris(mu-phthalazine)dicopper(I) bis(trifluoromethanesulfonate), [Cu2(C6H 5CN)2(i-phtz)3][CF3SO 3]2 (7), was established from {[Cu(CF3SO 3)]2 ¡¤C6H5Me}, phthalazine and benzonitrile via the very air-sensitive intermediate [Cu2(CF 3SO3)2(mu-phtz)3] (6). Copper(I) compounds 2, 4, and 7 were completely characterised and the molecular structures confirmed in the solid state by single-crystal X-ray structure determination. The analysis of the packing of the molecules in crystals of 4 and 7 revealed a self-assembly of oneand three-dimensional frameworks, respectively, resulting from intermolecular pi-pi stacking interactions between pyridazine-type ligands.
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Reference£º
Phthalazine – Wikipedia,
Phthalazine | C8H6N343 – PubChem