An article Fluorocyclization of N-Propargylamides to Oxazoles by Electrochemically Generated ArIF2 WOS:000489200100044 published article about DOPED DIAMOND ELECTRODES; FLUORINATION; AMIDES; CYCLOISOMERIZATION; CATALYSIS; ELECTROSYNTHESIS; CYCLIZATION; ASCIDIANS; REAGENTS; SEQUENCE in [Herszman, John D.; Berger, Michael; Waldvogel, Siegfried R.] Johannes Gutenberg Univ Mainz, Inst Organ Chem, Duesbergweg 10-14, D-55128 Mainz, Germany in 2019.0, Cited 62.0. Name: 4-Nitrobenzoic acid. The Name is 4-Nitrobenzoic acid. Through research, I have a further understanding and discovery of 62-23-7
A sustainable synthesis of 5-fluoromethyl-2-oxazoles by use of electrochemistry has been demonstrated. Hypervalent ArIF2 is generated by direct electrochemical oxidation of iodoarene ArI in Et3N center dot 5HF and mediates the fluorocyclization of N-propargylamides to 5-fluoromethyl-2-oxazoles. The stoichiometry in ArI turned out to be a key parameter in controlling the product selectivity. This electrochemical protocol provides access to fluorinated oxazoles starting from simply available N-propargylamides with yields up to 65% and offers a green alternative over conventional reagent-based approaches.
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Reference:
Phthalazine – Wikipedia,
,Phthalazine | C8H6N2 – PubChem