369-34-6, Name is 3,4-Difluoronitrobenzene, molecular formula is C6H3F2NO2, belongs to phthalazines compound, is a common compound. In a patnet, author is Milenkovic, Milica, once mentioned the new application about 369-34-6, HPLC of Formula: C6H3F2NO2.
Synthesis, characterization and crystal structures of Ni(II) and Cu(I) complexes with the condensation product of 2-(diphenylphosphino) benzaldehyde and 1-hydrazinophthalazine
A square-pyramidal Ni(II) complex (1) with the composition [NiL(HL’)]CIO4 center dot H2O was synthesized in the reaction of nickel(II) perchlorate and 2[2-(diphenylphosphino)benzylidene]-1-phthalazinylhydrazone (HL). The coordination surrounding the Ni(II) ion consist of a PNN coordinated deprotonated HL ligand and its corresponding oxidation product phosphine oxide HL’ coordinated via two nitrogen atoms of the hydrazinophthalazine moiety. The structure of Ni(II) complex 1 was determined by X-ray analysis, IR spectroscopy, elemental analysis and magnetic measurements. In the reaction of copper(II) perchlorate with HL, a binuclear phthalazine bridged Cu(I) complex (2) was obtained with the composition [Cu-2(HL)(2)](ClO4)(2)center dot C2H5OH. The structure of Cu(I) complex 2 was determined by X-ray analysis, IR and NMR spectroscopy, elethental analysis and magnetic measurements. (C) 2016 Elsevier Ltd. All rights reserved.
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Reference:
Phthalazine – Wikipedia,
,Phthalazine | C8H6N2 – PubChem